Chem. Heterocycl. Compd. 2019, 55 (2), 189‑192
DOI: 10.1007/s10593-019-02438-0
Mykhaylychenko S.; Markitanov Y.; Rudenko T.; Rusanov E.; Shermolovich Y.
New 4-polyfluoroalkyl-1,3-dithiolanes were synthesized by reaction of polyfluoroalkanethioamides with thiocarbonyl ylide that was generated in situ by desilylation of chloromethyl (trimethylsilyl)methyl sulfide with tetramethylammonium fluoride.
![Synthesis of 4-polyfluoroalkyl-1,3-dithiolanes via [3+2] cycloaddition of thiocarbonyl ylide to polyfluoroalkanethioamides](/images/publications/2019/10.1007_s10593-019-02438-0.PNG)