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Eur. J. Org. Chem. 2019, (23), 3744-3750

DOI: 10.1002/ejoc.201900485

Martyloga O.; Myronenko A.; Tkachenko A.; Matvienko V.; Kuchkovska Y.; Grygorenko O.

An approach to the synthesis of spirocyclic diazirines from cyclic ketones was examined on a series of carbo‐ and heterocyclic substrates containing the amine or carboxylic acid moiety. A mini‐library of stereochemically diverse functionalized spirocyclic diazirines was synthesized on a multigram scale with 30–81 % yield.

Multigram Synthesis of Functionalized Spirocyclic Diazirines

 

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